Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 178486040, 화합물 → HCID 178486042, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 178486040 | HCID 178486040 | — |
| 촉매 | Platinum dioxide monohydrate | HCID 11139377 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178486042 | HCID 178486042 | 101.4% |
반응 단계
A suspension of 3.4 g (12.72 mmol) of trans-[4-(3-Hydroxy-prop-1-ynyl)-cyclohexyl]-methyl-carbamic acid tert-butyl ester in 125 ml ethanol and 810 mg of PtO2.H2O was hydrogenated (1 atm) for 7 h. The reaction was filtered (Celite) and evaporated to give 3.5 g (quantitative) of trans-[4-(3-Hydroxy-propyl)-cyclohexyl]-methyl-carbamic acid tert-butyl ester, MS: 271 (MH).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06858651B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-29e6230aee9c4456978ce0d50f9c6058 |
| 출처 메모 | uspto-grants-2005_02 |