Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,7-Naphthalenediol → 2,7-Bis(propargyloxycarbonyloxy)naphthalene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,7-Naphthalenediol | HCID 11397 | — |
| 반응물 | Propargyl chloroformate | HCID 3356829 | — |
| 생성물 | 2,7-Bis(propargyloxycarbonyloxy)naphthalene | HCID 19786013 | 83.6% |
반응 단계
Analogous to Example 19, 2,7-dihydroxynaphthalene was reacted with propargyl chloroformate to produce the title compound. Yield was 83.6% theory. m.p. 94°-96° C. IR (cm-1) 3330, 2100, 1755, 1610, 1510 1H-NMR (δ, ppm) 2.42 (CH≡C--), 4.86 (≡C--CH2 --), 7.20, 8.10 (Ph)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05258542 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-424109b6790244448c38f1f5d44e923b |
| 출처 메모 | uspto-grants-1993_11 |