Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diisobutylaluminumhydride → 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]styrol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diisobutylaluminumhydride | HCID 21225700 | — |
| 반응물 | 2,3,Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styryl carboxylate | HCID 131719753 | — |
| 생성물 | 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]styrol | HCID 18359165 | 99.6% |
반응 단계
Using the procedure of Stage C of Example 40, 20 g of ester of Step B and 88 ml of diisobutylaluminium hydride were reacted to obtain 17.9 g of the expected product melting at 60° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728828 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-3a2ecc42a142468888fdaba3359f6ee1 |
| 출처 메모 | uspto-grants-1998_03 |