Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Norbornene-2-carboxylic acid → Bicyclo[2.2.1]heptane-2-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Norbornene-2-carboxylic acid | HCID 78949 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Bicyclo[2.2.1]heptane-2-carboxylic acid | HCID 79113 | 94% |
반응 단계
15.7 g (110 mmol) of crude 5-norbornene-2-carboxylic acid was dissolved in 300 ml of ethanol, 1.55 g of 5% palladium-carbon powder was added, and the mixture was stirred under an atmosphere of hydrogen for 24 hours. After the catalyst was filtered off, the solvent was distilled off, and 14.5 g of crude 2-norbornanecarboxylic acid was obtained. Crude yield: 94%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05266728 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-450580ae0ff94758a4f9e307b836054b |
| 출처 메모 | uspto-grants-1993_11 |