Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetonitrile → 1-Butylpiperazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetonitrile | HCID 6342 | — |
| 반응물 | 2-(7-Chloro-1,8-naphthyridin-2-yl)-3-phenoxycarbonyloxy-1-isoindolinone | HCID 23343637 | — |
| 생성물 | 1-Butylpiperazine | HCID 424322 | — |
반응 단계
Following the procedure of Example 15 but starting with 2-(7-chloro-1,8-naphthyridin-2-yl)-3-phenoxycarbonyloxy-isoindolin-1-one (5.1 g.) and 1-t.-butylpiperazine (5 g.) in acetonitrile (31 cc.), 2-(7-chloro-1,8-naphthyridin-2-yl)-3-(4-t.-butylpiperazin-1-yl)carbonyloxy-isoindolin-1-one (3.3 g.), melting at 240° C., is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04038391 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-ccaf40d687bd4d68af52336ab49e1b83 |
| 출처 메모 | uspto-grants-1977_07 |