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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 260830생성일: 2026년 10월 24일

Hydrochloric Acid → 12-(Benzyloxy)-12-oxododecanoic acid

https://huagongshe.com/ko/reaction/260830

반응식

참여 물질

역할이름HCID투입량
반응물Hydrochloric AcidHCID 313—
반응물Benzyl BromideHCID 7498—
반응물Potassium CarbonateHCID 11430—
반응물Dodecanedioic AcidHCID 12736—
용매DimethylformamideHCID 6228—
용매Ethyl AcetateHCID 8857—
생성물12-(Benzyloxy)-12-oxododecanoic acidHCID 14250267—

반응 단계

A mixture of 1,10-decanedicarboxylic acid, benzyl bromide and potassium carbonate in N,N-dimethylformamide was stirred at room temperature for 16 hours. The reaction mixture was poured into a mixture of ethyl acetate and diluted hydrochloric acid, and the organic layer was washed with water and brine, dried over magnesium sulfate and concentrated. The residue was chromatographed on a silica gel column to give the object compound.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05530019
출처 데이터셋uspto-grants-1996_06
ORD IDord-9e3afd87bc3a4568953de2b65dff0663
출처 메모uspto-grants-1996_06