Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isopropanol → 3-(4-Chloro-3-sulfamoylbenzoyl)-1,2-dimethylindole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isopropanol | HCID 3776 | — |
| 반응물 | 1,2-Dimethylindole | HCID 13408 | — |
| 반응물 | 3-(Aminosulfonyl)-4-chlorobenzoyl chloride | HCID 3017979 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 용매 | 1,1-Dichloroethane | HCID 6365 | — |
| 생성물 | 3-(4-Chloro-3-sulfamoylbenzoyl)-1,2-dimethylindole | HCID 21316638 | — |
반응 단계
is obtained as described in Example 10 (a) from 10 g 4-chloro-3-sulfamoylbenzoyl chloride and 6.53 g 1,2-dimethylindole in dichloro-ethane in the presence of 12 g aluminum chloride. After treatment with isopropanol, crystals having a melting point of 247°-249° C. are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04156732 |
| 출처 데이터셋 | uspto-grants-1979_05 |
| ORD ID | ord-a3b045773a7b453484155875cccb118d |
| 출처 메모 | uspto-grants-1979_05 |