Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Gentisate → Methyl 5-(2-cyclohexylethoxy)-2-hydroxybenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Gentisate | HCID 75077 | — |
| 반응물 | 2-Cyclohexylethyl 4-methylbenzenesulfonate | HCID 11426070 | — |
| 생성물 | Methyl 5-(2-cyclohexylethoxy)-2-hydroxybenzoate | HCID 19036723 | 43% |
반응 단계
Synthesis was carried out in the same manner as in Example 1, except for replacing methyl 2,4-dihydroxybenzoate with methyl 2,5-dihydroxybenzoate and replacing 2-ethylhexyl bromide with 2-cyclohexylethyl p-toluenesulfonate, to obtain methyl 5-(2-cyclohexylethoxy)-2-hydroxybenzoate represented by the following chemical formula (hereinafter referred to as compound 11) as a pale yellow solid in a yield of 43%. The analytical results are shown below. ##STR32##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05646184 |
| 출처 데이터셋 | uspto-grants-1997_07 |
| ORD ID | ord-dde65f479bc54da9b6f090eb6743d7ff |
| 출처 메모 | uspto-grants-1997_07 |