Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 22314064, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | N-(2-Methoxyethyl)ethylamine | HCID 546877 | — |
| 반응물 | HCID 22313931 | HCID 22313931 | — |
| 반응물 | HCID 22314065 | HCID 22314065 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 22314064 | HCID 22314064 | — |
반응 단계
In analogy to example 3.1, 6-(4-Bromo-butoxy)-3-(4-bromo-phenyl)-benzo[d]isothiazole and N-(2-Methoxyethyl)ethylamine were converted to {4-[3-(4-Bromo-phenyl)-benzo[d]isothiazol-6-yloxy]-butyl}-ethyl-(2-methoxy-ethyl)-amine which was converted to the hydrochloride by treatment with HCl in methanol to yield {4-[3-(4-Bromo-phenyl)-benzo[d]isothiazol-6-yloxy]-butyl}-ethyl-(2-methoxy-ethyl)-amine hydrochloride as light yellow oil, MS: 463(MH+, 1Br).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07449483B2 |
| 출처 데이터셋 | uspto-grants-2008_11 |
| ORD ID | ord-349c7ea7eb594fed8e4695d0d8cc7c61 |
| 출처 메모 | uspto-grants-2008_11 |