Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosgene → 2,6-Dimethylpiperidine-1-carbonyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosgene | HCID 6371 | — |
| 반응물 | Nanofin | HCID 68843 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 2,6-Dimethylpiperidine-1-carbonyl chloride | HCID 19070661 | — |
반응 단계
To a solution of 50 g of 2,6-dimethylpiperidine in 300 ml of benzene is added 60 g of phosgene and the mixture is refluxed for 3 hours. The solid which had separated was filtered and the filtrate was concentrated and distilled under vacuum to obtain 2,6-dimethylpiperidinoyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04220658 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-d11774a1636640a29040ec7cd02bfe95 |
| 출처 메모 | uspto-grants-1980_09 |