Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N-Dimethylaniline → HCID 13753447, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N-Dimethylaniline | HCID 949 | — |
| 반응물 | 4-Ethoxyaniline | HCID 9076 | — |
| 반응물 | 2,6-Dichloro-3-nitrobenzoic acid | HCID 350623 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | HCID 13753447 | HCID 13753447 | — |
반응 단계
A mixture of 28.0 g of p-phenetidine, 23.6 g of 2,6-dichloro-3-nitrobenzoic acid, and 80 ml of N,N-dimethylaniline was heated five hours on a steam bath. The resulting mixture was diluted with chloroform and extracted with 1N sodium hydroxide. Acidification of the aqueous extract yielded 6-chloro-2-[(4-ethoxyphenyl)amino]-3-nitrobenzoic acid as reddish brown crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04588730 |
| 출처 데이터셋 | uspto-grants-1986_05 |
| ORD ID | ord-f49559616c584729aba38e22075119ed |
| 출처 메모 | uspto-grants-1986_05 |