Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-(Trifluoromethoxy)benzenesulphonyl chloride → HCID 10095610, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-(Trifluoromethoxy)benzenesulphonyl chloride | HCID 523102 | — |
| 반응물 | (2-Amino-5-chlorophenyl)-pyridin-4-yl methanone | HCID 10214538 | — |
| 생성물 | HCID 10095610 | HCID 10095610 | — |
반응 단계
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using (2-amino-5-chloro-phenyl)-pyridin-4-yl-methanone and 4-Trifluoromethoxy-benzenesulfonyl chloride and purified by HPLC. 1H NMR (DMSO-d6): δ 6.90 (d, J=8.4 Hz, 1H), 7.50 (d, J=8.8 Hz, 2H), 7.49-7.61 (m, 4H), 7.66 (d, J=8.8 Hz, 2H), 8.81 (d, J=4.8 Hz, 2H), 10.26 (s, 1H). MS: M/z 456.9 (M++1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07420055B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-e3d81c7ce0da44458092b7aa5eb92849 |
| 출처 메모 | uspto-grants-2008_09 |