Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl isobutyrylacetate → HCID 178439455, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl isobutyrylacetate | HCID 81583 | — |
| 반응물 | 3-Nitrobenzamidinium hydrochloride | HCID 12456162 | — |
| 생성물 | HCID 178439455 | HCID 178439455 | — |
반응 단계
The title compound was prepared from 4-methyl-3-oxo-pentanoic acid ethyl ester and 3-nitro-benzamidine hydrochloride according to general procedure 1. 1H NMR (DMSO-d6, 400 MHz) δ 1.25 (d, J=6.9 Hz, 6H), 2.80-2.92 (m, 1H), 6.37 (s, 1H), 7.83 (t, J=8.0 Hz, 1H), 8.40 (dd, J=7.5, 2.3 Hz, 2H), 8.62 (d, J=7.5 Hz, 1H) 9.01 (s, 1H), 12.50 (br s, 1H); MS: m/z (ESI) 260 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423044B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-707a9d40dbf140d3a49b0d0c7fe2cce2 |
| 출처 메모 | uspto-grants-2008_09 |