Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Chloroaniline → 3-(3-Chlorophenylamino)-6-oxo-7-phenyl-6,7-dihydrothieno[2,3-b]pyridine-2-carbonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Chloroaniline | HCID 7932 | — |
| 반응물 | 6-Oxo-7-phenyl-3-phenylamino-6,7-dihydro-thieno[2,3-b]pyridine-2-carbonitrile | HCID 68457647 | — |
| 생성물 | 3-(3-Chlorophenylamino)-6-oxo-7-phenyl-6,7-dihydrothieno[2,3-b]pyridine-2-carbonitrile | HCID 68455562 | — |
반응 단계
The title compound was prepared from 3-chloroaniline (115 mg, 0.9 mmol) following the method described for the compound of Example 18 to give the product as a pale yellow solid (125 mg). δH (CDCl3) 7.67-7.58 (3H, m), 7.44-7.41 (2H, m), 7.39 (1H, d, J 9.7 Hz), 7.31-7.26 (1H, m), 7.12-7.09 (1H, m), 7.04 (1H, t, J 2.0 Hz), 6.95-6.92 (1H, m), 6.57 (1H, d, J 9.7 Hz), 6.54 (1H, bs). LCMS (ES+) 378 (M+H)+35Cl, 380 (M+H)+37Cl.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423047B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-f1ed07b14a674593aab6b4f661d3500e |
| 출처 메모 | uspto-grants-2008_09 |