Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(5-Bromo-3-pyridinyl)methanol → 5-Bromo-3-pyridinecarboxaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (5-Bromo-3-pyridinyl)methanol | HCID 2784733 | — |
| 촉매 | Manganese dioxide | HCID 14801 | — |
| 생성물 | 5-Bromo-3-pyridinecarboxaldehyde | HCID 2784734 | 51.1% |
반응 단계
(5-Bromo-pyridin-3-yl)-methanol (1.13 g, 6.00 mmol) was dissolved in CHCI3 (40 mL) and treated with MnO2 (3.60 g). The reaction mixture was heated at reflux temperature for 3 h. The hot reaction mixture was filtered through a pad of diatomaceous earth and the filtrate was concentrated to yield the title compound (0.570 g, 51%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423147B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-a363896c2f4243088d27486a0d5c3e7a |
| 출처 메모 | uspto-grants-2008_09 |