Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Imidazoline → 1-(4-Ethylphenyl)-2-imidazolylethan-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Imidazoline | HCID 68156 | — |
| 반응물 | 2-Bromo-1-(4-ethylphenyl)ethan-1-one | HCID 12401951 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 1-(4-Ethylphenyl)-2-imidazolylethan-1-one | HCID 22142578 | — |
반응 단계
1 mmol of 2-bromo-1-(4-ethylphenyl)ethan-1-one in acetonitrile was added drop wise to 5.5 mmol imidazoline in acetonitrile at room temperature for fourteen hours. The reaction mixture was concentrated in vacuo and diluted with water and ethyl acetate. The solution was extracted three times with ethyl acetate and dried over sodium sulfate to obtain 1-(4-ethylphenyl)-2-imidazolylethan-1-one.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07425557B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-24ee89c2f0684d92a2fe9090065cfceb |
| 출처 메모 | uspto-grants-2008_09 |