참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2,6-Dimethylbenzoic acid | HCID 12439 | — |
| 생성물 | 2,6-Dimethyl-3-nitrobenzoic acid | HCID 239329 | — |
반응 단계
13.5 g (90.0 mmol) of 2,6-dimethylbenzoic acid were introduced in portions into a solution of 25 ml of conc. sulfuric acid and 25 ml of 65% strength HNO3 cooled to 0° C. After stirring at 0° C. for 1 h, the reaction mixture was poured onto ice, and the precipitate deposited was filtered off with suction and dried. 15.5 g of the title compound resulted.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06211196B1 |
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| 출처 데이터셋 | uspto-grants-2001_04 |
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| ORD ID | ord-790e5437b9c847eaaa58a676fb399b9e |
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| 출처 메모 | uspto-grants-2001_04 |
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