Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Dichloroacetone → 4-Chloromethyl-2-(3,5-dimethylphenyl)oxazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Dichloroacetone | HCID 10793 | — |
| 반응물 | 3,5-Dimethylbenzamide | HCID 319485 | — |
| 생성물 | 4-Chloromethyl-2-(3,5-dimethylphenyl)oxazole | HCID 22009628 | 52% |
반응 단계
In substantially the same manner as in Reference Example 31, 3,5-dimethylbenzamide was allowed to react with 1,3-dichloroacetone to give 4-chloromethyl-2-(3,5-dimethylphenyl)oxazole. The yield was 52%. Recrystallization from isopropyl ether gave colorless needles, mp 76-77° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06211215B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-3ab89e7985c0403891800f8cfb004588 |
| 출처 메모 | uspto-grants-2001_04 |