Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → tert-Butyl 4-(2-methoxy-2-oxoethyl)piperidine-1-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Tert-butyl 4-(2-methoxy-2-oxoethylidene)piperidine-1-carboxylate | HCID 10377658 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | tert-Butyl 4-(2-methoxy-2-oxoethyl)piperidine-1-carboxylate | HCID 1514280 | 99.9% |
반응 단계
tert-Butyl 4-(2-methoxy-2-oxoethylidene)piperidine-1-carboxylate (3.6 g, 14 mmol) and 10% Pd/C moistered with water (0.8 g) was mixed in MeOH (75 mL) and stirred under H2 (1 atm) for 4 h. The mixture was filtered through Celite and concentrated to give the title compound (3.6 g, 99%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07427631B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-48d486ba3dc64acaae68325a2655a90a |
| 출처 메모 | uspto-grants-2008_09 |