Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methyluracil → HCID 178432331, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methyluracil | HCID 12009 | — |
| 반응물 | 2-Methyl-1-(4-methoxyphenylmethyl)-4H-benzo[5,6]cyclohepta[1,2-d]imidazol-4-ol | HCID 22003671 | — |
| 용매 | Trifluoroacetic acid | HCID 6422 | — |
| 생성물 | HCID 178432331 | HCID 178432331 | — |
반응 단계
A stirred solution of the product from step (iii) (0.819 g) in trifluoroacetic acid (20 ml) was heated at reflux for 1 h. 1-Methyluracil (0.311 g) was added and the reflux continued for 5 days. The solvent was evaporated under reduced pressure. The residue was purified by chromatography eluting with 10% methanol in dichloromethane to give the subtitle product as pale green glass.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06218376B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-a866e5d4415144668ea8de1cb16098af |
| 출처 메모 | uspto-grants-2001_04 |