Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 2,4,5-Trimethyl-3-furancarbonyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2,4,5-Trimethylfuran-3-carboxylic acid | HCID 7131507 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2,4,5-Trimethyl-3-furancarbonyl chloride | HCID 14535934 | — |
반응 단계
2,4,5-Trimethyl-3-furancarbonyl chloride was prepared by refluxing 2,4,5-trimethyl-3-furancarboxylic acid (20.0 g) with thionyl chloride (20 ml) in toluene (75 ml) for 3 hours. The toluene and excess thionyl chloride were removed on a rotary evaporator and the residue distilled (b.p. 95°-97° C. at ca. 12 mm).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05268389 |
| 출처 데이터셋 | uspto-grants-1993_12 |
| ORD ID | ord-6e3063683a874e328e6fedbea747620b |
| 출처 메모 | uspto-grants-1993_12 |