Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzene → 2,3-Dichlorophenyl sulfamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzene | HCID 241 | — |
| 반응물 | 2,3-Dichlorophenol | HCID 11334 | — |
| 반응물 | Chlorosulfonyl isocyanate | HCID 70918 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2,3-Dichlorophenyl sulfamate | HCID 54352588 | 72% |
반응 단계
This compound was prepared according to the procedure of Example 84. Thus, a mixture of 16.3 g (0.10 mole) of 2,3-dichlorophenol and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 75 ml of toluene gave 17.4 g (72%) of the title compound as an off-white solid, mp 116°-117° C. (benzene).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05273993 |
| 출처 데이터셋 | uspto-grants-1993_12 |
| ORD ID | ord-90931d6a25ac4c54a78f345978ebacff |
| 출처 메모 | uspto-grants-1993_12 |