Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl 9-bromononanoate → (E)-9-[3-(6-Hydroxy-1-hexynyl)-2-(3-methoxy-3-oxo-1-propenyl)phenoxy]nonanoic Acid Methyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl 9-bromononanoate | HCID 554142 | — |
| 반응물 | (E)-3-[2-Hydroxy-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic Acid Methyl Ester | HCID 67780365 | — |
| 생성물 | (E)-9-[3-(6-Hydroxy-1-hexynyl)-2-(3-methoxy-3-oxo-1-propenyl)phenoxy]nonanoic Acid Methyl Ester | HCID 67780053 | 71% |
반응 단계
Using the procedure of example 122, (E)-3-[2-hydroxy-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic acid methyl ester (example 176) was alkylated with methyl 9-bromononanoate giving the title compound, in 71% yield, as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05273999 |
| 출처 데이터셋 | uspto-grants-1993_12 |
| ORD ID | ord-814f389ddb484e6f8281e2277c0c2323 |
| 출처 메모 | uspto-grants-1993_12 |