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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 328061생성일: 2026년 10월 24일

Methanol → Triphenyl tin methoxide

https://huagongshe.com/ko/reaction/328061

반응식

참여 물질

역할이름HCID투입량
반응물MethanolHCID 887—
반응물Sodium ChlorideHCID 5234—
반응물Triphenyltin ChlorideHCID 12540—
반응물SodiumHCID 5360545—
용매TetrahydrofuranHCID 8028—
생성물Triphenyl tin methoxideHCID 23451602—

반응 단계

115.5 g of triphenyl tin chloride are dissolved in a mixture of 450 g of absolute methanol and 300 g of absolute tetrahydrofuran and mixed with a solution of 7.02 g of sodium in 150 ml of absolute methanol. After stirring for 2 hours at room temperature the resulting precipitate of sodium chloride is filtered off. The solution of triphenyl tin methoxide obtained is combined, accompanied by stirring, with a solution of 600 g of the epoxy resin modified with diketene described in Example 2 dissolved in 300 g of absolute tetrahydrofuran. After stirring for a further 2 hours at room temperature and after distilling off the solvent 696 g of a reddish brown glassy solid product of formula VI above are obtained. Tin content: calculated 5.51%; found 5.45%.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04016141
출처 데이터셋uspto-grants-1977_04
ORD IDord-daa566e319864535b88c11e65a57de7e
출처 메모uspto-grants-1977_04