Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 54171156, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Ethyl benzoylacetate | HCID 7170 | — |
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | (4-Chlorophenyl)(oxo)acetaldehyde | HCID 269588 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | HCID 54171156 | HCID 54171156 | — |
반응 단계
A solution containing 13.5 g of 4-chloro-phenylglyoxal and 15.4 g of ethyl benzoylacetate in 100 ml of anhydrous benzene was heated at the boiling temperature in the presence of a catalytic amount of piperidine (0.3 ml), till complete azeotropic distillation of the water formed during the reaction (about 6 hours).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04894384 |
| 출처 데이터셋 | uspto-grants-1990_01 |
| ORD ID | ord-ccbc51db34fc43bcab41e2e449c85992 |
| 출처 메모 | uspto-grants-1990_01 |