Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Vanillin → N-benzyloxycarbony-D-valine isopropylamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Vanillin | HCID 1183 | — |
| 반응물 | Isopropylamine | HCID 6363 | — |
| 반응물 | N-alpha-Benzyloxycarbonyl-D-valine | HCID 712434 | — |
| 용매 | Ethyl acetate hexane | HCID 21226206 | — |
| 생성물 | N-benzyloxycarbony-D-valine isopropylamide | HCID 14723623 | — |
반응 단계
Reaction of N-benzyloxycarbonyl-D-valine with isopropylamine by the method of Example 20, Part A afforded a quantitative yield of N-benzyloxycarbonyl-D-valine isopropylamide of R 0.61 (TLC, ethyl acetate/hexane, 1:1, vanillin spray).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04894464 |
| 출처 데이터셋 | uspto-grants-1990_01 |
| ORD ID | ord-4c3e69659dee44c18274040f6b2db3d0 |
| 출처 메모 | uspto-grants-1990_01 |