Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenol → Phenyl 3-(o-tolyl)propanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenol | HCID 996 | — |
| 반응물 | 3-(2-Methylphenyl)propanoyl chloride | HCID 13029201 | — |
| 생성물 | Phenyl 3-(o-tolyl)propanoate | HCID 86715420 | 93% |
반응 단계
The procedure as described in Example 4a) was repeated with phenol (48 mmol) and 3-o-tolylpropanoyl chloride (55 mmol). The crude product (12.4 g, 97%) was short path distilled at 127-129° C./0.05 mbar to yield 10.6 g (93%) of product as a colourless, semicrystalline oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08877704B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-653a29921ad541cd957e9893431a59c5 |
| 출처 메모 | uspto-grants-2014_11 |