Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → Trimethoxyphenylsilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | 1-Butanol | HCID 263 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | Isopropanol | HCID 3776 | — |
| 반응물 | Tetraethoxysilane | HCID 6517 | — |
| 반응물 | Phenyltriethoxysilane | HCID 13075 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Trimethoxyphenylsilane | HCID 18137 | — |
반응 단계
In a 1-liter flask 297 grams (4.798 moles) 2-propanol, 148 grams (2.558 moles) acetone, 123 grams (0.593 moles) TEOS, 104 grams (0.432 moles) phenyltriethoxysilane, 0.6 grams 0.1 M, 0.01 M and 1.0 M nitric acid (added to three separate solutions, respectively) and 72 grams deionized water were combined. In two other solutions containing 0.1 M nitric acid, 90 g and 110 g of deionized water were added, respectively. The flask was refluxed and/or heated for 1 to 12 hours. To the solution, 57 grams (0.769 moles) of Butanol, 88 grams (1.422 moles) 2-propanol, 44 grams (0.758 moles) of acetone, 59 grams (1.227 moles) of ethanol, 9.5 grams (0.528 moles) deionized water were added.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08889334B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-eadfda233a9b441e9c430b35affe88e0 |
| 출처 메모 | uspto-grants-2014_11 |