참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Hydroxyethyl acrylate | HCID 13165 | — |
| 반응물 | 2,6-Di-tert-butyl-4-methylphenol | HCID 31404 | — |
| 반응물 | N,N',N''-Tris(3-dimethylaminopropyl)hexahydro-S-triazine | HCID 85160 | — |
| 반응물 | Isocyanate | HCID 105034 | — |
| 반응물 | 3-(Methylthio)phenyl isocyanate | HCID 141418 | — |
| 생성물 | 2-(((3-(Methylsulfanyl)phenyl)carbamoyl)oxy)ethyl prop-2-enoate | HCID 59273262 | — |
반응 단계
0.02 g of 2,6-di-tert-butyl-4-methylphenol, 0.01 g of Desmorapid® Z, 11.7 g of 3-(methylthio)phenyl isocyanate were initially introduced and initially introduced into a 100 ml round-bottomed flask and heated to 60° C. Thereafter, 8.2 g of 2-hydroxyethyl acrylate were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Cooling was then effected. The product was obtained as a light yellow liquid. nD20:1.626.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08889321B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_11 |
|---|
| ORD ID | ord-07b85c56bd1d447aa6d3d4b972c1e8b6 |
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| 출처 메모 | uspto-grants-2014_11 |
|---|
