Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Heptanamine → 1-(2,4-Dimethoxyphenyl)-3-(heptan-4-yl)urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Heptanamine | HCID 38665 | — |
| 반응물 | 2,4-Dimethoxyphenyl isocyanate | HCID 601637 | — |
| 생성물 | 1-(2,4-Dimethoxyphenyl)-3-(heptan-4-yl)urea | HCID 11300877 | 88% |
반응 단계
Prepared in a similar manner to example 158 using heptan-4-amine and 1-isocyanato-2,4-dimethoxybenzene. Yield: 88%. mp: 172-173° C. 1H NMR (500 MHz, CDCl3): δ 0.93 (t, 6H), 1.45 (m, 8H), 3.82 (s, 3H), 3.83 (m, 1H), 3.84 (s, 1H), 4.32 (br s, 1H), 6.34 (br s, 1H), 6.49 (d, 1H), 6.50 (s, 1H), 7.71 (d, 1H). MS (M+H, 295).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08895050B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-596fb7c9758347f181c2cf4244652118 |
| 출처 메모 | uspto-grants-2014_11 |