참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 1-Piperidineacetic acid, ethyl ester | HCID 643466 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-(Piperidin-1-yl)acetohydrazide | HCID 6421769 | — |
반응 단계
3.86 g of piperidin-1-yl-acetic acid ethyl ester was dissolved in 40 mL of ethanol, added with 3.39 mL of hydrazine monohydrate, and stirred at 70° C. for 5 hours. After allowing the solution to cool to room temperature, the solvent was evaporated, to afford 3.8 g of the title compound as pale yellow crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07429609B2 |
|---|
| 출처 데이터셋 | uspto-grants-2008_09 |
|---|
| ORD ID | ord-c7ae76d9cb824d00b70c01074d2b137b |
|---|
| 출처 메모 | uspto-grants-2008_09 |
|---|
