Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylhydrazine → 1-Boc-1-methylhydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylhydrazine | HCID 6061 | — |
| 반응물 | Di-tert-butyl dicarbonate | HCID 90495 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-Boc-1-methylhydrazine | HCID 3748280 | — |
반응 단계
10 mL of methyl hydrazine was dissolved in 90 mL of ethanol, and under stirring at ice-cooling, a solution of 41 g of di-tert-butyldicarbonate in 90 mL of ethanol was added dropwise over 45 minutes. After stirring at room temperature for 7 hours, the solvent was evaporated, to afford 24.7 g of the title compound as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07429609B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-fc6875eeb4de43a8bab93f777795ac96 |
| 출처 메모 | uspto-grants-2008_09 |