Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dicyclohexylcarbodiimide → HCID 178444553, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 반응물 | 4-Hydroxyphenylsulfur pentafluoride | HCID 2779203 | — |
| 반응물 | HCID 178444557 | HCID 178444557 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178444553 | HCID 178444553 | — |
반응 단계
A mixture of 10.6 g of dicyclohexylcarbodiimide and 40 ml of methylene chloride is added to a mixture of 9.1 g of trans-4-pentylcyclohexylcarboxylic acid, 11.2 g of p-hydroxyphenyl-sulfur pentafluoride and 100 ml of methylene chloride, and the combined mixture is heated at the boil for 6 hours. Working up in the customary manner gives 4-(trans-4-pentylcyclohexylcarbonyloxy)-phenyl-sulfur pentafluoride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05055223 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-f36d29740ac64520a38116d18d5930db |
| 출처 메모 | uspto-grants-1991_10 |