Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Phenoxybenzaldehyde → 5,5-Dimethyl-2-(3-phenoxyphenyl)-3-(4-phenylbutyl)-4-thiazolidinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Phenoxybenzaldehyde | HCID 38284 | — |
| 반응물 | 2-Mercapto-2-methylpropanoic acid | HCID 78421 | — |
| 반응물 | Benzenebutanamine | HCID 83242 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 5,5-Dimethyl-2-(3-phenoxyphenyl)-3-(4-phenylbutyl)-4-thiazolidinone | HCID 19990602 | — |
반응 단계
Using the procedures of Example 5, the title compound was prepared as a light yellow viscous oil (8.4 g, 65%) from 5.9 g (0.030 mole) of 3-phenoxybenzaldehyde (Fluka), 3.6 g (0.030 mole) of 2-mercapto-2-methylpropionic acid, and 4.6 g (0.030 mole) of 4-phenylbutylamine after refluxing in 250 ml of benzene overnight.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05061720 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-79c0bbcc9ca8426eb94a9eff610b6370 |
| 출처 메모 | uspto-grants-1991_10 |