Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzenamine, 2-phenoxy- → 1-Isothiocyanato-2-phenoxybenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzenamine, 2-phenoxy- | HCID 75899 | — |
| 반응물 | Thiocarbonyl diimidazole | HCID 11412697 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-Isothiocyanato-2-phenoxybenzene | HCID 22040439 | — |
반응 단계
1.96 g (0.011 mol) of thiocarbonyl diimidazole were added to a solution of 1.85 g (0.01 mol) of 2-phenoxyaniline in 50 ml of THF and the mixture was stirred at room temperature for 4 hours, giving, after removal of the solvent by distillation, the compound as a brown amorphous product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07179829B2 |
| 출처 데이터셋 | uspto-grants-2007_02 |
| ORD ID | ord-853bee71781a42c6a85dc3d3c78adb8d |
| 출처 메모 | uspto-grants-2007_02 |