Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Imidazole → HCID 23511477, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Imidazole | HCID 795 | — |
| 반응물 | tert-Butyldimethylsilane | HCID 5072427 | — |
| 반응물 | 4-(Hydroxymethyl)-5-methyl-1,3-dioxol-2-one | HCID 10510878 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 23511477 | HCID 23511477 | — |
반응 단계
A solution of 5-methyl-4-hydroxymethyl-2-oxo-1,3-dioxolene (1 mmole) in DMF was treated with tert-butyldimethylsilane (1.2 mmole) and imidazole (2.2 mmole) at 25° C. for 24 h. Extraction and chromatography gave 5-methyl-4-tert-butyldimethylsilyloxymethyl-2-oxo-1,3-dioxolene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06756360B1 |
| 출처 데이터셋 | uspto-grants-2004_06 |
| ORD ID | ord-e740a62547524ca48f9b5d1ddf9d1883 |
| 출처 메모 | uspto-grants-2004_06 |