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HRID 359144생성일: 2026년 10월 24일

1-(4-Chlorophenyl)-1-octen-3-one → 1-(4-Chlorophenyl)-3-octanone

https://huagongshe.com/ko/reaction/359144

반응식

참여 물질

역할이름HCID투입량
반응물1-(4-Chlorophenyl)-1-octen-3-oneHCID 54522967—
촉매NickelHCID 935—
용매TolueneHCID 1140—
생성물1-(4-Chlorophenyl)-3-octanoneHCID 1453761096.4%

반응 조건

온도60 °C

반응 단계

15 g of Raney nickel are added to a solution of 100 g (0.423 mol) of 1-(4-chlorophenyl)-1-octen-3-one in 500 ml of toluene and the mixture is stirred for 5 hours at 60° C. under a hydrogen pressure of 70-90 bar in an autoclave. After this the reaction mixture is filtered and concentrated under reduced pressure. 97.3 g (96.4% of theory) of 1-(4-chlorophenyl)-3-octanone are obtained in the form of a colorless oil. ##STR36##

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04999440
출처 데이터셋uspto-grants-1991_03
ORD IDord-52fb2ce33c404f84a31b8d431707be5d
출처 메모uspto-grants-1991_03