Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Anthranilamide → N-[(2-carbamoylphenyl)carbamothioyl]-3-methylbenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Anthranilamide | HCID 6942 | — |
| 반응물 | 3-Methylbenzoyl isothiocyanate | HCID 141397 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | N-[(2-carbamoylphenyl)carbamothioyl]-3-methylbenzamide | HCID 667545 | 89.3% |
반응 단계
To a stirred mixture of 7.2 g of 2-aminobenzamide and 200 ml of ether was added dropwise, a solution of 10 g of 3-methylbenzoyl isothiocyanate over 10 minutes. After 48 hours, the solid was collected, giving 14.8 g of the desired product as grey crystals, mp 194°-196° (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05001157 |
| 출처 데이터셋 | uspto-grants-1991_03 |
| ORD ID | ord-0d79b3cbfe21472dbe9de27f6fa957f8 |
| 출처 메모 | uspto-grants-1991_03 |