Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → 3-Acetyl-1-(p-acetamidophenyl)-3-azabicyclo[3.1.0]hexane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 3-Acetyl-1-(p-aminophenyl)-3-azabicyclo[3.1.0]hexane | HCID 20468332 | — |
| 용매 | Sodium Diacetate | HCID 23662384 | — |
| 생성물 | 3-Acetyl-1-(p-acetamidophenyl)-3-azabicyclo[3.1.0]hexane | HCID 20352249 | — |
반응 단계
A solution of 3-acetyl-1-(p-aminophenyl)-3-azabicyclo[3.1.0]hexane in aqueous acetic acid-sodium acetate is treated with acetic anhydride at ambient temperature. The reaction mixture is chilled and filtered to give 3-acetyl-1-(p-acetamidophenyl)-3-azabicyclo[3.1.0]hexane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04088652 |
| 출처 데이터셋 | uspto-grants-1978_05 |
| ORD ID | ord-f94df4f344024768bd329a144a2703ea |
| 출처 메모 | uspto-grants-1978_05 |