Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(Pyridin-2-yl)propan-1-amine → HCID 178512789, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(Pyridin-2-yl)propan-1-amine | HCID 3159614 | — |
| 반응물 | S-methyl isothiourea hemisulfate | HCID 6604939 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178512789 | HCID 178512789 | — |
반응 단계
A solution of 2-(3-aminopropyl)pyridine (2.72 g) and S-methylthiouronium sulphate (2.78 g) in water (40 ml) is heated under reflux for 28 hours. The product isolated by the manner described in Example 1 was recrystallized from methanol, yielding 3-(2-pyridyl)propylguanidine sulphate, m.p. 185°-187° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04088769 |
| 출처 데이터셋 | uspto-grants-1978_05 |
| ORD ID | ord-7f50331ed03b4f5c90002a3e7ae7bccd |
| 출처 메모 | uspto-grants-1978_05 |