Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 178419936, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 2-Naphthalenecarbonitrile | HCID 11944 | — |
| 반응물 | Sodium Azide | HCID 33557 | — |
| 반응물 | Lithium Chloride | HCID 433294 | — |
| 용매 | 2-Methoxyethanol | HCID 8019 | — |
| 생성물 | HCID 178419936 | HCID 178419936 | — |
반응 단계
A mixture of 10 g of 2-cyanonaphthalene, 10.61 g of sodium azide, and 7.67 g of lithium chloride was placed in a reaction vessel, and 240 ml of 2-methoxyethanol serving as a solvent was added thereto. The above mixture was refluxed with stirring for 80 hours. The mixture was cooled to room temperature, and 500 ml of water was added to the mixture.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05420288 |
| 출처 데이터셋 | uspto-grants-1995_05 |
| ORD ID | ord-28f1ea35b4c54d3e98646f4aae82b802 |
| 출처 메모 | uspto-grants-1995_05 |