Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → Sodium 4-allyloxyphenylsulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Allyl bromide | HCID 7841 | — |
| 반응물 | Sodium benzenesulfonate | HCID 517327 | — |
| 용매 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | Sodium 4-allyloxyphenylsulfonate | HCID 86748076 | — |
반응 단계
30 g of sodium phenylsulfonate are dissolved in 60 ml of ethanol and 50 ml of 15% sodium hydroxide, 20 g of allyl bromide are added and the mixture is refluxed for 48 hours. The ethanol is concentrated and the precipitate obtained is filtered off and then dried under vacuum in the presence of phosphorus pentoxide to give 23.3 g of the expected product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05481005 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-a77c4c4bb86f4f6896706e2d2950ecd9 |
| 출처 메모 | uspto-grants-1996_01 |