Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethylamine → Benzoic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethylamine | HCID 8021 | — |
| 반응물 | 2-Chloro-5-(fluorosulpho)benzoic acid | HCID 88873 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | Benzoic Acid | HCID 243 | — |
반응 단계
A mixture of 2-chloro-5-(fluorosulfonyl)benzoic acid (11.93 g, 0.05 mol), diethylamine (10.97 g, 0.15 mol) and 1,2-dichloroethane (100 mL) was refluxed for 8 hours. The reaction mixture was evaporated and the residue was dissolved in ethyl acetate. A solid was collected by filtration and the filtrate was evaporated to dryness to afford 15.5 g of 2-chloro-5-diethylaminosulfonyl)benzoic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05488055 |
| 출처 데이터셋 | uspto-grants-1996_01 |
| ORD ID | ord-498b6d423ed8427fba6d206335405625 |
| 출처 메모 | uspto-grants-1996_01 |