Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl bromide → 2-(2-(Allyloxy)ethoxy)ethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl bromide | HCID 7841 | — |
| 반응물 | Diethylene Glycol | HCID 8117 | — |
| 용매 | NaH THF | HCID 23694757 | — |
| 생성물 | 2-(2-(Allyloxy)ethoxy)ethanol | HCID 84777 | 82% |
반응 단계
Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08524104B1 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-4e69885985a74b1ca4a5f8fc798f2882 |
| 출처 메모 | uspto-grants-2013_09 |