Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitrogen → Di-tert-butyl ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitrogen | HCID 947 | — |
| 반응물 | tert-Butanol | HCID 6386 | — |
| 반응물 | 1-Hexanol | HCID 8103 | — |
| 반응물 | Hexyl t-butyl ether | HCID 547839 | — |
| 생성물 | Di-tert-butyl ether | HCID 22541 | — |
반응 단계
300 mmoles of t-butanol, 100 mmoles of 1-hexanol and 2.5 g of Ti-Si-catalyst powder are stirred in a 100 ml autoclave at a pressure of 40 bar N2 and a temperature of 150° C. over a period of 17 h, 17% of n hexanol were converted into hexyl t-butyl ether with a selectivity of 90%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06297180B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-c4b88dc8fc2f43d4a6be06585468b591 |
| 출처 메모 | uspto-grants-2001_10 |