참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 2-Chloroquinoxaline | HCID 238938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Hydrazinoquinoxaline | HCID 289847 | — |
반응 단계
15.0 g (91.1 mmol) of 2-chloroquinoxaline are initially charged in 150 ml of ethanol. 45.6 g (911.3 mmol) of hydrazine hydrate are added, and the mixture is stirred under reflux for 16 h. The mixture is then cooled to 0° C., and the solid formed is filtered off, washed with ethanol and dried under high vacuum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08524699B2 |
|---|
| 출처 데이터셋 | uspto-grants-2013_09 |
|---|
| ORD ID | ord-efc7ff43d5da4470838ac669ec7ef138 |
|---|
| 출처 메모 | uspto-grants-2013_09 |
|---|
