Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Cyclohexyl-3-(2-morpholinoethyl)carbodiimide metho-p-toluenesulfonate → HCID 10514281, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Cyclohexyl-3-(2-morpholinoethyl)carbodiimide metho-p-toluenesulfonate | HCID 17220 | — |
| 반응물 | 4,5-Dichloro-1,2-phenylenediamine | HCID 79297 | — |
| 반응물 | Cyclopropyl isothiocyanate | HCID 92463 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 10514281 | HCID 10514281 | 70.5% |
반응 단계
4,5-Dichloro-1,2-phenylenediamine (6.04 g, 34.1 mmol), cyclopropyl isothiocyanate (3.69 g, 37.2 mmol), 1-cyclohexyl-3-(2-morpholinoethyl)carbodiimide metho-p-toluenesulfonate (20.1 g, 47.4 mmol) and pyridine (135 mL) were used according to general procedure I. The product was recrystallized from acetonitrile to afford 5.82 g (70%) of a yellow solid; m.p. 223-225° C. Anal. Calcd for C10H9Cl2N3: C, 49.61; H, 3.75; N, 17.36. Found: C, 49.53; H, 3.78; N, 17.12.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06307043B1 |
| 출처 데이터셋 | uspto-grants-2001_10 |
| ORD ID | ord-7822d9433a7a4c408cecd83ed668d803 |
| 출처 메모 | uspto-grants-2001_10 |