Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexyl isocyanate → HCID 178418539, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexyl isocyanate | HCID 75659 | — |
| 반응물 | 3-[4-(4-Chlorobenzyl)piperazin-1-yl]propanethiol | HCID 13731117 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178418539 | HCID 178418539 | 157.9% |
반응 단계
The procedure described in Example 35 was followed, using 1.4 g of n-hexyl isocyanate, 3.0 g of 3-[4-(4-chlorobenzyl)piperazin-1-yl]propanethiol and 100 ml of methylene chloride, to give 2.7 g (51% of theory) of N-(n-hexyl)-S-{3-[4-(4-chlorobenzyl)piperazin-1-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, M.p. 249°-252° C. (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04722926 |
| 출처 데이터셋 | uspto-grants-1988_02 |
| ORD ID | ord-b3cce434c6ef4afc85c9dbb95a837744 |
| 출처 메모 | uspto-grants-1988_02 |