Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-1-propene-1,1,3-tricarbonitrile → (E,E)-2-(1-Amino-2,2-dicyanoethenyl)-3-(4-nitrostyryl)acrylonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-1-propene-1,1,3-tricarbonitrile | HCID 13356 | — |
| 반응물 | 3-(4-Nitrophenyl)prop-2-enal | HCID 15614 | — |
| 생성물 | (E,E)-2-(1-Amino-2,2-dicyanoethenyl)-3-(4-nitrostyryl)acrylonitrile | HCID 86588371 | — |
반응 단계
The compound was prepared as described in Example 3 by adding 4-nitrocinnamaldehyde (0.051 g, 0.29 mmol) to 2-amino-1-propene-1,1,3-tricarbonitrile (0.038 g, 0.29 mmol). After refluxing for 4 h and recrystallization from ethanol a yellow solid was obtained (0.08 g, 51%). The product gave the following analytical data:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06800659B2 |
| 출처 데이터셋 | uspto-grants-2004_10 |
| ORD ID | ord-f7bdd87b05274d70a960490cd9a1527e |
| 출처 메모 | uspto-grants-2004_10 |