Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperidine → Glycyl-phenylalanyl-glycine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | N-Fmoc-glycyl-L-phenylalanyl-glycine | HCID 15222489 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Glycyl-phenylalanyl-glycine | HCID 6992441 | — |
반응 단계
Fmoc-protected tripeptide 74 (546 mg, 0.98 mmol) was treated with a 5% v/v solution of piperidine in DMF (5 mL). After stirring for 45 min, the reaction mixture was concentrated to dryness. The crude material was used for the next step without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08524691B2 |
| 출처 데이터셋 | uspto-grants-2013_09 |
| ORD ID | ord-7e66b13904154ebcbe524b75757fe2f1 |
| 출처 메모 | uspto-grants-2013_09 |